HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20484846, compound → HCID 20484852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20484846 | HCID 20484846 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20484852 | HCID 20484852 | 93.3% |
Reaction Steps
A suspension of 1.5 g of manganese dioxide in 50 ml of methylene chloride was stirred under an inert gas for 15 minutes and 200 mg of the product of Step C were added. The mixture was stirred for one hour and was filtered. The filtrate was evaporated to dryness to obtain 185 mg of ethyl 3,3-dimethyl-5-(2-hydroxy-2-methyl-propyl)-[3H]-pyrazole-4-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04299973 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-51602cda830148f39ff789f53766e23c |
| Source note | uspto-grants-1981_11 |