HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethylaniline → 3,4-Dimethyl-N-phenylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethylaniline | HCID 7248 | — |
| Reactant | 3,5-Dimethylaniline | HCID 7949 | — |
| Product | 3,4-Dimethyl-N-phenylaniline | HCID 14958605 | 84% |
Reaction Steps
The procedure of Example IV is repeated with the exception that 3,4-dimethylaniline was substituted for 3,5-dimethylaniline. After a reaction time of 3.5 hours, the crude reaction product was recrystallized once from hexane to give an 84 percent yield of 3,4-dimethyldiphenylamine having a melting point of 55°-55.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04299983 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-2541082edb7c4cb1a172fd8b7f07eb72 |
| Source note | uspto-grants-1981_11 |