HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Hydroxide → Tributylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Tributylamine | HCID 7622 | — |
Reaction Steps
Three grams of coal liquid derived from Illinois No. 6 coal and having a boiling range of 340° to 565° C. was mixed with 8 cc of 2 M tetrabutylammonium hydroxide in methanol. The resulting quaternary ammonium organic salt was then heated to 250° C. A thermal rearrangement took place which produced an O-butylated coal liquid and tributylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04300995 |
| Source dataset | uspto-grants-1981_11 |
| ORD ID | ord-81007eb99dc34f2c8a959b97a1fef156 |
| Source note | uspto-grants-1981_11 |