5-(Chloromethyl)-1,2,3-trimethoxybenzene → HCID 12926476, compound

HRID 1155280Notes

Reaction equation

HRID 1155280 reaction equation
[C:1]1([C:7]([CH2:11][N:12]([CH3:14])[CH3:13])([OH:10])[CH2:8][CH3:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:15][O:16][C:17]1[CH:18]=[C:19]([CH2:27]Cl)[CH:20]=[C:21]([O:25][CH3:26])[C:22]=1[O:23][CH3:24]>>[CH3:26][O:25][C:21]1[CH:20]=[C:19]([CH:18]=[C:17]([O:16][CH3:15])[C:22]=1[O:23][CH3:24])[CH2:27][O:10][C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)([CH2:8][CH3:9])[CH2:11][N:12]([CH3:14])[CH3:13]

Participants

3

Reactant 2

HCID 774485-(Chloromethyl)-1,2,3-trimethoxybenzeneHCID 205616591-(Dimethylamino)-2-phenylbutan-2-ol

Product 1

HCID 12926476HCID 12926476, compound

Procedure

Prepared according to the process described in Example 3 from 1-phenyl-1-dimethylaminomethyl-1-propanol and from 3,4,5-trimethoxy-α-chlorotoluene.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f2a37d4c152146009de7334ec72f16c0
Source dataset
uspto-grants-1981_11
Patent number
US04301163

Reaction notes

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