Sulfuryl chloride → HCID 53650123, compound

Participants

Reaction Steps

To 6.8 g of O-methyl S-methyl N-(2-methylphenylsulfonyl)carbonimidothioate in 20 ml of methylene chloride is added 6.8 g of sulfuryl chloride. The reaction mixture is stirred under a nitrogen atmosphere at ambient temperature for 2 hours, and then refluxed for an additional 2 hours. Removal of the solvent under reduced pressure gives 5.0 g of methyl N-(2-methylphenylsulfonyl)carbonimidochloridate as a light yellow oil. This product is used without further purification in the reaction described in Example 3.

Provenance & Evidence