Ethanol → HCID 13470385, compound

HRID 1155527Notes

Reaction equation

HRID 1155527 reaction equation
[C:1]([C:5]1[CH:14]=[C:13]2[C:8]([C:9](=[O:19])[C:10]([S:16]([CH3:18])=[O:17])=[CH:11][N:12]2[CH3:15])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].C([OH:22])C>C(Cl)(Cl)Cl>[C:1]([C:5]1[CH:14]=[C:13]2[C:8]([C:9](=[O:19])[C:10]([S:16]([CH3:18])(=[O:22])=[O:17])=[CH:11][N:12]2[CH3:15])=[CH:7][CH:6]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

4

Reactant 2

HCID 702EthanolHCID 13470357HCID 13470357, compound

Product 1

HCID 13470385HCID 13470385, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

7-t-butyl-1-methyl-3-methylsulphinyl-4-quinolone was oxidised in chloroform at 20° to give 7-t-butyl-1-methyl-3-methylsulphonyl-4-quinolone, m.p. 247°-248° (from ethanol).

Sources & evidence

ORD record
ord-55ca28b0f141416f9b38487340b87c9b
Source dataset
uspto-grants-1981_11
Patent number
US04302460

Reaction notes

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