Ethanol → HCID 20561002, compound
Reaction equation
[CH3:1][N:2]1[C:11]2[C:6](=[CH:7][CH:8]=[C:9]([CH:12]([CH3:14])[CH3:13])[CH:10]=2)[C:5](=[O:15])[C:4]([S:16][CH3:17])=[CH:3]1.C([OH:20])C>>[CH3:1][N:2]1[C:11]2[C:6](=[CH:7][CH:8]=[C:9]([CH:12]([CH3:13])[CH3:14])[CH:10]=2)[C:5](=[O:15])[C:4]([S:16]([CH3:17])=[O:20])=[CH:3]1Participants
3
Procedure
Similarly, the compound 1-methyl-3-methylthio-7-isopropyl-4-quinolone of Example 13 was oxidised to give the compound 1-methyl-3-methylsulphinyl-7-isopropyl-4-quinolone, m.p. 214°-215° (from ethanol).
Sources & evidence
- ORD record
- ord-80c223152f2f4dd7807a1c315d757fce
- Source dataset
- uspto-grants-1981_11
- Patent number
- US04302460
Reaction notes
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