Ethyl propanecarboximidate hydrochloride → HCID 178463245, compound

HRID 1155550Notes

Reaction equation

HRID 1155550 reaction equation
[CH2:1]([NH:3][C:4]1[CH:9]=[C:8]([C:10](OCC)(OCC)[CH2:11][NH2:12])[CH:7]=[CH:6][N:5]=1)[CH3:2].Cl.[C:20](=[NH:26])(OCC)[CH2:21][CH3:22]>C(O)C>[CH2:1]([NH:3][C:4]1[CH:9]=[C:8]([C:10]2[N:26]=[C:20]([CH2:21][CH3:22])[NH:12][CH:11]=2)[CH:7]=[CH:6][N:5]=1)[CH3:2]

Participants

4

Reactant 2

HCID 13000588Ethyl propanecarboximidate hydrochlorideHCID 131452922-(2-Ethylamino-4-pyridyl)-2,2-diethoxyethylamine

Product 1

HCID 178463245HCID 178463245, compoundYield 33%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The procedure of Example XB was employed, starting with 2.0 g. (8 mmoles) of 2-(2-ethylamino-4-pyridyl)-2,2-diethoxyethylamine and 1.16 g. (8.3 mmoles) of ethyl propionimidate hydrochloride in 30 ml. of ethanol, to give 605 g. (33%) of the title compound as a white solid, 190°-193° C.

Sources & evidence

ORD record
ord-62ade12b9a1d46ce98da697bcae22026
Source dataset
uspto-grants-1981_11
Patent number
US04302464

Reaction notes

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