HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1155653Generated: October 31, 2026
Adipic Acid → Sodium silicate vinyl chloride propylene oxide
https://huagongshe.com/reaction/1155653
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Adipic Acid | HCID 196 | — |
| Reactant | Vinyl Chloride | HCID 6338 | — |
| Reactant | Propylene Oxide | HCID 6378 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Sodium orthosilicate | HCID 26051 | — |
| Reactant | Sodium Stearate | HCID 2724691 | — |
| Product | Sodium silicate vinyl chloride propylene oxide | HCID 86738391 | — |
Reaction Steps
About 50 parts by weight of an aqueous sodium silicate solution containing about 15% Na2O and 25% SiO2 by weight, 10 parts by weight of propylene oxide, 2 parts by weight of adipic acid, 0.2 parts by weight of sodium stearate and 0.1 part by weight of benzoyl peroxide are mixed then added to an autoclave and a temperature of about 50° C. is maintained at a pressure between 7.0 and 7.1 kg per cm2. Vinyl chloride monomer is slowly added while agitating over a period of 7 to 10 hours until the emulsion contains about 30% vinyl chloride polymerized with the sodium silicate and propylene oxide thereby producing an emulsion of poly(sodium silicate-vinyl chloride-propylene oxide) copolymer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04332712 |
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| Source dataset | uspto-grants-1982_06 |
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| ORD ID | ord-e307f394e1d14a248edf8a933ba47284 |
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| Source note | uspto-grants-1982_06 |
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