HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-3-methyl-2-butene → 52750-95-5
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-3-methyl-2-butene | HCID 10429 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 52750-95-5 | HCID 18954555 | 80.5% |
Reaction Steps
A stirred solution of 52.3 g (0.5 mole) of 3-methyl-2-butenyl chloride and 144.1 g (0.55 mole) of triphenylphosphine in 400 ml of toluene was heated at 100° C. for 18 hours. The white solid formed was collected by filtration to give 147.6 g of (3-methyl-2-butenyl)triphenylphosphonium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332815 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-5fcfdb11168b43eaaa19e790f8214bb8 |
| Source note | uspto-grants-1982_06 |