Triethylamine → Methylthiomethyl 2-Methyl-2-pentenoate

HRID 1155726노트

반응식

HRID 1155726 반응식
[CH3:1][C:2](=[CH:6][CH2:7][CH3:8])[C:3]([OH:5])=[O:4].[CH3:9][S:10][CH2:11]Cl.C(N(CC)CC)C>>[CH3:1][C:2](=[CH:6][CH2:7][CH3:8])[C:3]([O:5][CH2:9][S:10][CH3:11])=[O:4]

참가 물질

4

반응물 3

HCID 8471TriethylamineHCID 16916Chloromethyl methyl sulfideHCID 184582-Methylpent-2-en-1-oic acid

생성물 1

HCID 54484466Methylthiomethyl 2-Methyl-2-pentenoate

실험 절차

This product was prepared according to the procedure described in Example 1, by reacting 2-methyl-2-pentenoic acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 56°-57° C./2 mm Hg, nD20 1.4861.

후처리

  1. customThis product was prepared

출처 및 근거

ORD 기록
ord-67783be822b14d6f8248176a2484e91b
출처 데이터셋
uspto-grants-1982_06
특허 번호
US04332829

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