HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → 3-(3-Methoxyphenyl)butyltriphenylphosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 1-Bromo-3-(3-methoxyphenyl)butane | HCID 20496919 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 3-(3-Methoxyphenyl)butyltriphenylphosphonium bromide | HCID 20496878 | — |
Reaction Steps
The 3-(3-methoxyphenyl)butyltriphenylphosphonium bromide is prepared by refluxing a mixture of 1-bromo-3-(3-methoxyphenyl)butane (78.5 mmoles) and triphenyl phosphine (78.5 mmoles) in xylene (60 ml.) for 18 hours. The reaction mixture is then cooled to room temperature and filtered. The filter cake is washed with ether and the product dried in a vacuum desiccator.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04332942 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-630067a4616340ea8c60905174ae91b7 |
| Source note | uspto-grants-1982_06 |