HRID1156015

反应详情

EQUATION

反应方程式

HRID 1156015 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

The latter nitro derivative (17.0 g) in 500 ml of methanol was reduced at room temperature and pressure with hydrogen using 4 g of 10% palladium on carbon as catalyst for 6 hr and filtered. The solvent was removed to give 14 g of 2-amino-3,4,5-trimethoxybenzoic acid methyl ester as an oil.

WORKUP

后处理

  1. customwas reduced at room temperature
  2. filtrationfiltered
  3. customThe solvent was removed