Piperidine, 1-methyl-4-(4-nitrophenoxy)-4-phenyl- → 4-(4-Nitrophenoxy)-4-phenylpiperidine

HRID 1156032Notes

Reaction equation

HRID 1156032 reaction equation
C[N:2]1[CH2:7][CH2:6][C:5]([O:14][C:15]2[CH:20]=[CH:19][C:18]([N+:21]([O-:23])=[O:22])=[CH:17][CH:16]=2)([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH2:4][CH2:3]1.C(OC(N1CCC(OC2C=CC([N+]([O-])=O)=CC=2)(C2C=CC=CC=2)CC1)=O)C>>[N+:21]([C:18]1[CH:17]=[CH:16][C:15]([O:14][C:5]2([C:8]3[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=3)[CH2:4][CH2:3][NH:2][CH2:7][CH2:6]2)=[CH:20][CH:19]=1)([O-:23])=[O:22]

Participants

3

Reactant 2

HCID 3060390Piperidine, 1-methyl-4-(4-nitrophenoxy)-4-phenyl-HCID 20536581HCID 20536581, compound

Product 1

HCID 200299564-(4-Nitrophenoxy)-4-phenylpiperidine

Procedure

(oil), from 1-methyl-4-(4-nitrophenoxy)-4-phenylpiperidine, intermediate 1-ethoxycarbonyl-4-(4-nitrophenoxy)-4-phenylpiperidine of m.p. 137° to 138° C.

Sources & evidence

ORD record
ord-0a61528d4e1145e39089e61f0cdac5b6
Source dataset
uspto-grants-1982_06
Patent number
US04333942

Reaction notes

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