HCID 20199818, compound → HCID 20199821, compound

Participants

Reaction Steps

To a slurry of 11.8 grams (0.044 mole) of 3-methylthio-6-methyl-4-phenylindoline-2-one in 500 milliliters of tetrahydrofuran are added 100 grams of a commercial Raney nickel/water preparation portionwise over a two-hour period. The mixture is filtered through Celite and the filtrate concentrated. A small amount of methylene chloride is added to the residue and the resulting solid is collected by filtration.

Provenance & Evidence