HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20199723, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Tin atom | HCID 5352426 | — |
| Reactant | HCID 20199643 | HCID 20199643 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20199723 | HCID 20199723 | — |
Reaction Steps
A mixture of 4.9 grams (0.014 mole) of 3-methylthio-4-phenyl-5,7-dinitroindolin-2-one, 4.2 grams (0.035 mole) of tin powder, 10 milliliters of concentrated hydrochloric acid and 50 milliliters of ethanol are refluxed for 4 hours under nitrogen. The hot mixture is filtered and the filtrate concentrated to give a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04333951 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-d8392204ab3143bbb605ada611d43575 |
| Source note | uspto-grants-1982_06 |