Acrylonitrile → HCID 54152861, compound

HRID 1156070Notes

Reaction equation

HRID 1156070 reaction equation
[C:1]([CH2:3][CH2:4][O:5]CCOC(O)C)#N.[C:12](#[N:15])[CH:13]=[CH2:14].[CH2:16]([OH:22])[CH2:17][O:18][CH2:19][CH2:20][OH:21]>>[C:4]([O:22][CH2:16][CH2:17][O:18][CH2:19][CH2:20][O:21][CH2:14][CH2:13][C:12]#[N:15])(=[O:5])[CH:3]=[CH2:1]

Participants

4

Reactant 3

HCID 7855AcrylonitrileHCID 8117Diethylene GlycolHCID 131712754HCID 131712754, compound

Product 1

HCID 54152861HCID 54152861, compound

Procedure

Following the procedures described in Example 1, cyanoethoxyethoxyethanol (bp 144°-151° C./2 mm Hg) is prepared from diethylene glycol and acrylonitrile, acrylation of which gives the desired product.

Sources & evidence

ORD record
ord-d05174291e5f4040828aedd67014bbe7
Source dataset
uspto-grants-1982_06
Patent number
US04333963

Reaction notes

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