Acrylonitrile → HCID 22413884, compound

HRID 1156072Notes

Reaction equation

[C:1]([CH2:3][CH2:4][O:5][CH2:6][CH2:7][CH2:8][CH2:9][OH:10])#[N:2].C(O)[CH2:12][CH2:13][CH2:14][OH:15].C(#N)C=C>>[C:14]([O:10][CH2:9][CH2:8][CH2:7][CH2:6][O:5][CH2:4][CH2:3][C:1]#[N:2])(=[O:15])[CH:13]=[CH2:12]

Participants

Reactant 3

HCID 7855Acrylonitrile

HCID 80641,4-Butanediol

HCID 134165593-(4-Hydroxybutoxy)propanenitrile

Product 1

HCID 22413884HCID 22413884, compound

Procedure

Following the procedures described in Example 1, 4-(2-cyanoethoxy)-1-butanol (bp 148°-152° C./4.5 mm Hg) is prepared from 1,4-butanediol and acrylonitrile, acrylation of which gives the desired product.

Sources & evidence

ORD record: ord-86f0e293ed2d4775a6e9ce1c19a282cf
Source dataset: uspto-grants-1982_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04333963

Reaction notes

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