Acrylonitrile → HCID 20536718, compound

HRID 1156073Notes

Reaction equation

HRID 1156073 reaction equation
[C:1]([CH2:3][CH2:4][O:5][CH:6]([CH3:10])[CH2:7][CH2:8][OH:9])#[N:2].[CH2:11](O)[CH2:12][CH:13]([OH:15])C.C(#N)C=C>>[C:13]([O:9][CH2:8][CH2:7][CH:6]([O:5][CH2:4][CH2:3][C:1]#[N:2])[CH3:10])(=[O:15])[CH:12]=[CH2:11]

Participants

4

Reactant 3

HCID 7855AcrylonitrileHCID 78961,3-ButanediolHCID 20536719HCID 20536719, compound

Product 1

HCID 20536718HCID 20536718, compound

Procedure

Following the procedures described in Example 1, 3-(2-cyanoethoxy)-1-butanol (bp 145°-150° C./2.5 mm Hg) is prepared from 1,3-butanediol and acrylonitrile, acrylation of which gives the desired product.

Sources & evidence

ORD record
ord-0b17e1faaef4466bb60c2699eafb8c46
Source dataset
uspto-grants-1982_06
Patent number
US04333963

Reaction notes

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