Sodium Hydroxide → HCID 23709242, compound

HRID 1156182Notes

Reaction equation

HRID 1156182 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][C:13](=[O:17])[C:14]([OH:16])=[O:15])=[CH:5][CH:4]=1.[OH-].[Na+:19]>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][C:13](=[O:17])[C:14]([O-:16])=[O:15])=[CH:7][CH:8]=1.[Na+:19]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 20537158HCID 20537158, compound

Product 1

HCID 23709242HCID 23709242, compound

Procedure

4.5 g of 6-(4-methoxyphenyl)-2-oxo-caproic acid in 19.0 ml of 1 N sodium hydroxide solution are stirred for 15 minutes at room temperature. The mixture is filtered, washed once with diethyl ether and evaporated to dryness. The residue obtained after drying in vacuo at 30° consists of the pure sodium salt.

Workup

  1. filtrationThe mixture is filtered
  2. washwashed once with diethyl ether
  3. customevaporated to dryness
  4. customThe residue obtained
  5. customafter drying in vacuo at 30°

Sources & evidence

ORD record
ord-a69d2db1598c40719d360a80683d4abd
Source dataset
uspto-grants-1982_06
Patent number
US04334089

Reaction notes

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