HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → p-BROMOPHENYL 1-(PHENYLSULFONYL)VINYL SULFIDE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-CHLORO-1-(PHENYLSULFONYL)ETHYL p-BROMOPHENYL SULFIDE | HCID 13044798 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | p-BROMOPHENYL 1-(PHENYLSULFONYL)VINYL SULFIDE | HCID 13044810 | — |
Reaction Steps
A solution of 10.2 g (26.1 mmoles) of 2-chloro-1-(phenylsulfonyl)ethyl p-bromophenyl sulfide in 50 ml of tetrahydrofuran was diluted with 50 ml of diethyl ether and treated with 3.63 ml (2.65 g, 26.2 mmoles) of triethylamine. After 20 minutes the triethylamine hydrochloride was removed by filtration. The filtrate was freed of solvent by evaporation under reduced pressure to leave a viscous, pale yellow oil of n20 1.6338.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04335142 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-ed20170bc6fc4bc284c0ff987a8d92c0 |
| Source note | uspto-grants-1982_06 |