10596-01-7 → HCID 20536090, compound

HRID 1156400Notes

Reaction equation

HRID 1156400 reaction equation
[CH2:1]([N:5]1[C:10]([OH:11])=[CH:9][C:8]([CH3:12])=[C:7]([C:13]#[N:14])[C:6]1=[O:15])[CH2:2][CH2:3][CH3:4].CC1C=CC=CC=1N(C)N=[O:21]>>[CH2:1]([N:5]1[C:6](=[O:15])[C:7]([C:13]#[N:14])=[C:8]([CH3:12])[C:9](=[O:21])[C:10]1=[O:11])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 4471933110596-01-7HCID 178448683HCID 178448683, compound

Product 1

HCID 20536090HCID 20536090, compound

Procedure

Prepared using the method of Example 2, with 1.03 g of 1-butyl-3-cyano-6-hydroxy-4-methylpyrid-2-one and 0.76 g of dimethyl-nitrosoaniline. Recrystallised from petrol/ethyl acetate, yield 0.54 g, m.p. 134°-135° C. This is the compound of formula (5).

Workup

  1. customPrepared
  2. customRecrystallised from petrol/ethyl acetate, yield 0.54 g, m.p. 134°-135° C

Sources & evidence

ORD record
ord-636ab329b7454f1089e35dac22d5b884
Source dataset
uspto-grants-1982_06
Patent number
US04335245

Reaction notes

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