HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Methacrylate → HCID 54322454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Methacrylate | HCID 7343 | — |
| Reactant | 4-Formylbenzoyl chloride | HCID 12424620 | — |
| Product | HCID 54322454 | HCID 54322454 | 29.4% |
Reaction Steps
The procedure described in Example 28 is repeated, except that 8.23 g (0.05 mol) of p-formylbenzoyl chloride and 7.13 g (0.0625 mol) of ethyl methacrylate are used. After a reaction time of 2 hours at 120° C., 3.2 g (0.0147 mol) of ethyl p-formyl-α-methylcinnamate are obtained, corresponding to a yield of 29.4% of theory; boiling point 127°-131° C./7 Pa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04335054 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-92bf1a8de0d343309b166b2cbab11855 |
| Source note | uspto-grants-1982_06 |