Ethylmorpholine → HCID 73028223, compound

Participants

Reaction Steps

0.0561 g (0.25 millimol) of palladium acetate, 5.76 g (25 millimols) of pentafluorobenzoyl chloride, 2.50 g (25 millimols) of ethyl acrylate and 2.88 g (25 millimols) of N-ethylmorpholine, in 100 ml of xylene, are stirred for 6.5 hours at 130° C. The crude product is distilled in vacuo. 3.9 g (59% of theory) of a colourless liquid (which distils at 61°-64° C./12 Pa) are obtained. Analysis for C11H7F5O2 : calculated C 49.64%, H 2.65%, F 35.69%; found C 49.76%, H 2.72%, F 35.90%.

Provenance & Evidence