Tributylamine → HCID 11264629, compound

Participants

Reaction Steps

0.2244 g (10-3 mols) of palladium acetate, 15.05 g (0.1 mol) of naphthalene-1-carboxylic acid chloride, 13.54 ml (0.125 mol) of ethyl acrylate and 23.95 ml (0.1 mol) of tri-n-butylamine, in 200 ml of p-xylene, are stirred for 1 hour at 120° C. The crude product is distilled in vacuo. 15.6 g (69% of theory) of a colourless liquid (which distils at 143°-147° C./106 Pa) are obtained. Analysis for C15H14O2 : calculated C 79.62%, H 6.24%, O 14.14%; found C 79.24%, H 6.39%, O 14.27%.

Provenance & Evidence