HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → HCID 54377318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | 4-Formylbenzoyl chloride | HCID 12424620 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Solvent | P-Xylene | HCID 7809 | — |
| Product | HCID 54377318 | HCID 54377318 | 8.4% |
Reaction Steps
3.91 mg (1.6×10-5 mols) of palladium acetate, 6.74 g (40 millimols) of 4-formylbenzoyl chloride, 2.63 ml (40 millimols) of acrylonitrile and 4.41 ml (40 millimols) of N-methylmorpholine, in 80 ml of p-xylene, are stirred for 5 hours. Working up as described in the preceding examples affords 0.53 g (8% of theory) of 4-formylcinnamonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04335054 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-fda5c4c5719a425c9a08601aa4706300 |
| Source note | uspto-grants-1982_06 |