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3-Methyltetrahydrofuran → 1,3-Dioxolane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methyltetrahydrofuran | HCID 98230 | — |
| 反応物 | 1,4-Dichloro-2-methylbutane | HCID 543860 | — |
| 反応物 | 3,4-Dimethyltetrahydrofuran | HCID 543880 | — |
| 反応物 | HCID 13561230 | HCID 13561230 | — |
| 生成物 | 1,3-Dioxolane | HCID 12586 | — |
| 生成物 | 1-Chloro-2-(chloromethoxy)ethane | HCID 10290810 | — |
反応手順
Using the reaction procedure described above, dimethyl carbonate is reacted with bis(1-chloro-2-propyl) ether to produce 2,6-dimethyl-p-dioxane, with 1,4-dichloro-2-methylbutane to make 3-methyltetrahydrofuran, with 1,4-dichloro-2,3-dimethylbutane to make 3,4-dimethyltetrahydrofuran, and with chloromethyl 2-chloroethyl ether to produce 1,3-dioxolane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04336195 |
| 出典データセット | uspto-grants-1982_06 |
| ORD ID | ord-b2b392aa7c6e4d598c4ff1b5146c3872 |
| 出典メモ | uspto-grants-1982_06 |