Isopropyl Palmitate → Nitroglycerin

HRID 1156505Notes

Reaction equation

HRID 1156505 reaction equation
[CH2:1]([O:12][N+:13]([O-:15])=[O:14])[CH:2]([O:8][N+:9]([O-:11])=[O:10])[CH2:3][O:4][N+:5]([O-:7])=[O:6].OC1O[C@H](CO)[C@@H](O[C@@H]2O[C@H](CO)[C@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@H]1O.C(OC(C)C)(=O)CCCCCCCCCCCCCCC>O>[CH2:3]([O:4][N+:5]([O-:7])=[O:6])[CH:2]([O:8][N+:9]([O-:11])=[O:10])[CH2:1][O:12][N+:13]([O-:15])=[O:14]

Participants

4

Reactant 2

HCID 8907Isopropyl PalmitateHCID 131712755HCID 131712755, compound

Product 1

HCID 4510Nitroglycerin

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Nitroglycerin pads (1.6×1.6 cm) were prepared following the method of Example 2 from 11 g of 10 percent nitroglycerin-lactose, labeled with C14 -nitroglycerin, 4.0 g of 10 percent (v/v) polyethylene glycol 400 in deionized water, 27.5 g of MDX 4-4210 silicone elastomer, 5.0 g of isopropyl palmitate and 2.5 of curing agent. The pads were stored in airtight containers.

Sources & evidence

ORD record
ord-ee2c62f38c594ac48e70229d4d2953ab
Source dataset
uspto-grants-1982_06
Patent number
US04336243

Reaction notes

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