2,6-Dichlorobenzoyl isocyanate → HCID 12960045, compound

HRID 1156533Notes

Reaction equation

HRID 1156533 reaction equation
[Cl:1][C:2]1[C:3]([NH2:17])=[N:4][O:5][C:6]=1[C:7]1[CH:12]=[CH:11][C:10]([C:13]([F:16])([F:15])[F:14])=[CH:9][CH:8]=1.[Cl:18][C:19]1[CH:29]=[CH:28][CH:27]=[C:26]([Cl:30])[C:20]=1[C:21]([N:23]=[C:24]=[O:25])=[O:22]>>[Cl:18][C:19]1[CH:29]=[CH:28][CH:27]=[C:26]([Cl:30])[C:20]=1[C:21]([NH:23][C:24]([NH:17][C:3]1[C:2]([Cl:1])=[C:6]([C:7]2[CH:12]=[CH:11][C:10]([C:13]([F:15])([F:14])[F:16])=[CH:9][CH:8]=2)[O:5][N:4]=1)=[O:25])=[O:22]

Participants

3

Reactant 2

HCID 129127392,6-Dichlorobenzoyl isocyanateHCID 12960075HCID 12960075, compound

Product 1

HCID 12960045HCID 12960045, compound

Procedure

4-Chloro-5-(4-(trifluoromethyl)phenyl)-3-aminoisoxazole was reacted with 2,6-dichlorobenzoyl isocyanate to produce the desired product according to the teaching of Example 8. The identity of the product was confirmed by NMR, m.p.=237°-238° C.

Sources & evidence

ORD record
ord-74383c2cfacc4625941e6468f0beb368
Source dataset
uspto-grants-1982_06
Patent number
US04336264

Reaction notes

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