Ammonia → HCID 70546287, compound
Reaction equation
Cl[CH2:2][CH2:3][O:4][Si:5]([CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)([CH3:7])[CH3:6].[NH3:16]>>[NH2:16][CH2:2][CH2:3][O:4][Si:5]([CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)([CH3:7])[CH3:6]Participants
3
Procedure
reacting said (chloromethyl) phenylethyldimethylmethoxysilane with ammonia under heat and pressure, and distilling the reaction mixture to yield (aminomethyl) phenylethyldimethylmethoxysilane.
Workup
- temperatureunder heat
- distillationpressure, and distilling the reaction mixture
Sources & evidence
- ORD record
- ord-919247755a8e4cab8b3a9786bea709f0
- Source dataset
- uspto-grants-1982_06
- Patent number
- US04336395
Reaction notes
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