HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl Phosphate → Triethyl phosphite
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl Phosphate | HCID 6535 | — |
| Catalyst | Tetramethylammonium chloride | HCID 6379 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Triethyl phosphite | HCID 31215 | — |
Reaction Steps
The electrolyte was 2.9 g. tetramethylammonium chloride in 60 ml anhydrous ethanol. The electrolysis was carried out at 35° C. for 88 hours at 6.5 v. to give 0.1 a current. Gas chromatographic analysis of the red-brown reaction liquor showed that both triethyl phosphate and triethyl phosphite were formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337125 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-e040cb1d5576452dbade08a6ee37d872 |
| Source note | uspto-grants-1982_06 |