Diphenyl disulfide → HCID 12851837, compound

HRID 1156881Notes

Reaction equation

HRID 1156881 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:18]3[C:13](=[C:14]([CH3:19])[CH:15]=[CH:16][CH:17]=3)[CH2:12][CH2:11][N:10]=2)=[CH:5][CH:4]=1.C1(SSC2C=CC=CC=2)C=CC=CC=1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:9]2[C:18]3[C:13](=[C:14]([CH3:19])[CH:15]=[CH:16][CH:17]=3)[CH:12]=[CH:11][N:10]=2)=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 13436Diphenyl disulfideHCID 12851823HCID 12851823, compound

Product 1

HCID 12851837HCID 12851837, compound

Procedure

1-(4-Methoxyphenyl)-5-methyl-3,4-dihydroisoquinoline and diphenyl disulfide were reacted in the same way as in step (c) of Example 1 to afford 1-(4-methoxyphenyl)-5-methylisoquinoline as colorless needles having a melting point of 60.4° to 60.8° C.

Sources & evidence

ORD record
ord-3ffbec8f0bb6498a95264b02deb2d540
Source dataset
uspto-grants-1982_06
Patent number
US04337256

Reaction notes

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