HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxide (P4O10) → 1-Cyclohexyl-5-chloro-3,4-dihydroisoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 1-Cyclohexylcarbonylamino-2-(2-chlorophenyl)ethane | HCID 12851819 | — |
| Product | 1-Cyclohexyl-5-chloro-3,4-dihydroisoquinoline | HCID 20533881 | — |
Reaction Steps
1-Cyclohexylcarbonylamino-2-(2-chlorophenyl)-ethane, phosphorus oxychloride and phosphorus pentoxide were reacted in the same was as in step (b) of Example 13 to afford 1-cyclohexyl-5-chloro-3,4-dihydroisoquinoline as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337256 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-f6f36ae2e2e44af59a73630a27a5a07d |
| Source note | uspto-grants-1982_06 |