HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 12802591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 12802589 | HCID 12802589 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12802591 | HCID 12802591 | — |
Reaction Steps
In 3 ml of acetic acid is dissolved 0.35 g of BOC-Tyr-(D)-Met-Gly-MePhe-NHNHCONH2 followed by addition of 0.082 ml of 30% aqueous H2O2. The solution is stirred for 10 minutes, treated with 100 ml of ether and filtered to obtain a powder. Yield 0.35 g (88%); m.p. 110°-115° C.; [α]D24 -35.1° (c=1.04, DMF); Rf1 0.05.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337247 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-99d0a1e1200546ed8e27bb1311f63a57 |
| Source note | uspto-grants-1982_06 |