HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-bromo-2-oxocyclohexanecarboxylate → Ethyl 2-methyl-4,5,6,7-tetrahydrobenzo[d]thiazole-4-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-bromo-2-oxocyclohexanecarboxylate | HCID 121765 | — |
| Reactant | Thioacetamide | HCID 2723949 | — |
| Product | Ethyl 2-methyl-4,5,6,7-tetrahydrobenzo[d]thiazole-4-carboxylate | HCID 12917740 | — |
Reaction Steps
This compound is prepared by action of thioacetamide on 2-bromo-6-carbethoxy-cyclohexanone (II), according to the process described in Example 1. B.p.0.1 =102°-105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337343 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-5aaace555378478783f266c723c12df2 |
| Source note | uspto-grants-1982_06 |