HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → 2-Methyl-6-tosyloxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 2-Methyl-6-hydroxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole | HCID 12917750 | — |
| Product | 2-Methyl-6-tosyloxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole | HCID 12917761 | 71% |
Reaction Steps
The compound is prepared by action of p-toluenesulfonyl chloride on the above derivative (IV) according to the procedure described in Example 1. M.p.=70°-71° C. Yield: 71%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337343 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-34a4179ae40342fb8463423659cd0244 |
| Source note | uspto-grants-1982_06 |