HCID 54026062, compound → HCID 20534485, compound

Participants

Reaction Steps

Hydrogen was passed through a solution of 2.07 g of the acid of Step A in 60 ml of methanol in the presence of 3 g of Raney nickel for 2 hours and the mixture was then filtered. The filtrate was evaporated to dryness and the residue was crystallized from isopropyl ether to obtain 1.328 g of 12-[3'-(4-chlorobenzoyl)-2'-methyl-phenyl]-dodecanoic acid melting at 79° C.

Provenance & Evidence