HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1157088Generated: November 2, 2026
HCID 59511048, compound → HCID 59511056, compound
https://huagongshe.com/reaction/1157088
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 59511048 | HCID 59511048 | — |
| Reactant | HCID 66850847 | HCID 66850847 | — |
| Product | HCID 59511056 | HCID 59511056 | — |
Reaction Steps
To a vial is added fluoroazide 17 (5.79 mmol) and 1-propynyl-2-nitroimidazole (5.79 mmol). The solution is heated at 60° C. overnight. The material is then purified on a silica gel column using EtOAc:Hex as the eluent. The material is then further purified via recrystallization using EtOAc:Hex to afford pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07807394B2 |
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| Source dataset | uspto-grants-2010_10 |
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| ORD ID | ord-425f22919fbe43d5b1b51fe388e54b05 |
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| Source note | uspto-grants-2010_10 |
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