HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzyloxy-5-nitro-biphenyl → 2-Biphenylol, 5-nitro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzyloxy-5-nitro-biphenyl | HCID 58985253 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Biphenylol, 5-nitro- | HCID 20278 | 65.4% |
Reaction Steps
To a solution of 2-benzyloxy-5-nitro-biphenyl (81 mg, 0.27 mmol)) in 5 mL of methanol was added catalytic amount of 5% palladium on carbon under H2. The mixture was stirred under H2 for 3 hrs and filtered through celite. The filtrate was concentrated to give 2-hydroxy-5-nitro-biphenyl (38 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07807672B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-be467441b133467eb389b365ed88e80a |
| Source note | uspto-grants-2010_10 |