HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → [3-Chloro-5-(3-chloro-5-cyanophenoxy)phenoxy]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | tert-Butyl[3-chloro-5-(3-chloro-5-cyanophenoxy)phenoxy]acetate | HCID 59511715 | — |
| Product | [3-Chloro-5-(3-chloro-5-cyanophenoxy)phenoxy]acetic acid | HCID 59511727 | — |
Reaction Steps
221 mg (0.561 mmol) of tert-butyl [3-chloro-5-(3-chloro-5-cyanophenoxy)phenoxy]acetate (5-2) was treated with neat trifluoroacetic acid until an LC/MS analysis indicated that the reaction was complete. The reaction was concentrated in vacuo and no further purification was done on the resultant desired product 5-3 which was isolated as an oil. MS: M+1=338.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07807684B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-424e6de3966f4c589662cbbc36eeda7c |
| Source note | uspto-grants-2010_10 |