HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octen-3-one → 1-[4-(3-Phenylpropyl)piperidin-1-yl]octan-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octen-3-one | HCID 61346 | — |
| Reactant | 4-(3-Phenylpropyl)piperidine | HCID 87678 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-[4-(3-Phenylpropyl)piperidin-1-yl]octan-3-one | HCID 11537237 | — |
Reaction Steps
1 equivalent of 4-(3-phenylpropyl)piperidine was reacted with 1 equivalent of 1-octen-3-one in ethanol, at room temperature. The product was worked up and purified on a column of silica. The results of the NMR and mass spectrometry analyses were in accordance with the expected structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07807695B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-b4a31479269c432a92e73378c7119399 |
| Source note | uspto-grants-2010_10 |