Butanoic acid, 2-bromo-, ethyl ester → HCID 178438252, compound

HRID 1157997Notes

Reaction equation

HRID 1157997 reaction equation
[CH2:1]1[CH2:6][CH2:5][CH:4]([NH:7][C:8]([NH2:10])=[S:9])[CH2:3][CH2:2]1.Br[CH:12]([CH2:18][CH3:19])[C:13](OCC)=[O:14]>>[CH:4]1([NH:7][C:8]2[S:9][CH:12]([CH2:18][CH3:19])[C:13](=[O:14])[N:10]=2)[CH2:5][CH2:6][CH2:1][CH2:2][CH2:3]1

Participants

3

Reactant 2

HCID 79039Butanoic acid, 2-bromo-, ethyl esterHCID 1471603Cyclohexylthiourea

Product 1

HCID 178438252HCID 178438252, compound

Procedure

Synthesis was performed from n-cyclohexylthiourea and ethyl 2-bromobutyrate according to Method C. Gave 201 mg (75%).

Workup

  1. customSynthesis
  2. customGave 201 mg (75%)

Sources & evidence

ORD record
ord-2e24e1ec9d5f418299ba2811ba6f5555
Source dataset
uspto-grants-2010_10
Patent number
US07807700B2

Reaction notes

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