Benzyl(cyclopropylmethyl)amine → N-Cyclopropylbenzenemethanamine

HRID 1158423Notes

Reaction equation

HRID 1158423 reaction equation

[CH2:1]([NH:8][CH2:9][CH:10]1[CH2:12]C1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(Cl)Cl.CO>[CH2:1]([NH:8][CH:9]1[CH2:10][CH2:12]1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 518069Benzyl(cyclopropylmethyl)amine

Product 1

HCID 25866N-Cyclopropylbenzenemethanamine

Reagents, catalysts & solvents 1

HCID 21226129Dichloromethane methanolSolvent

Procedure

The title compound is prepared analogously as described for benzyl-cyclopropylmethylamine. TLC, Rf (CH2Cl2/MeOH 95:5)=0.1, MS (LC-MS): 148.2 [M+H]+.

Sources & evidence

ORD record: ord-81ed3945ed394f9da1d55d342b0e0ccb
Source dataset: uspto-grants-2010_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07807709B2

Reaction notes

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