2-(Tributylstannyl)pyridine → HCID 11650493, compound

Participants

Reaction Steps

The title compound was prepared according to Method A, using compound 19 (100 mg, 0.147 mmol), 2-(1,1,1-tributylstannyl)pyridine (220 mg, 0.598 mmol), Pd(PPh)3Cl2 (5.12 mg, 0.0072 mmol) and CuO (11.7 mg, 0.147 mmol). Purification by RP-LC-MS (40 min gradient of 10-100% CH3CN in 0.05% aqueous formic acid) gave the product (17.2 mg, 17%) as a white solid.

Provenance & Evidence