3-(Tributylstannyl)pyridine → HCID 68678286, compound

Participants

Reaction Steps

The title compound was prepared according to Method A, using compound 19 (90.0 mg, 0.132 mmol), 3-(1,1,1-tributylstannyl)pyridine (194 mg, 0.527 mmol), Pd(PPh)3Cl2 (4.63 mg, 0.0065 mmol) and CuO (10.5 mg, 0.132 mmol). The product (24.0 mg, 27%) was afforded as a white solid after purification by RP-LC-MS (40 min gradient of 10-100% CH3CN in 0.05% aqueous formic acid).

Provenance & Evidence