Isopropanol → HCID 178457300, 화합물

HRID 1158604노트

반응식

HRID 1158604 반응식
[C:1]([S:14]([N:17]([CH2:21][CH2:22][CH2:23][C:24]([O:26]C)=[O:25])[CH2:18][CH2:19][CH3:20])(=[O:16])=[O:15])([C:4]([C:7]([C:10]([F:13])([F:12])[F:11])([F:9])[F:8])([F:6])[F:5])([F:3])[F:2].[OH-].[K+:29].C(O)(C)C>O>[C:1]([S:14]([N:17]([CH2:21][CH2:22][CH2:23][C:24]([O:26][K:29])=[O:25])[CH2:18][CH2:19][CH3:20])(=[O:16])=[O:15])([C:4]([C:7]([C:10]([F:13])([F:12])[F:11])([F:9])[F:8])([F:6])[F:5])([F:3])[F:2]

참가 물질

5

반응물 3

HCID 3776IsopropanolHCID 14797Potassium HydroxideHCID 131726673HCID 131726673, 화합물

생성물 1

HCID 178457300HCID 178457300, 화합물수율 163.2%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A round bottom flask fitted with a heating mantle and an overhead stirrer was charged with C4F9SO2N(C3H7)CH2CH2CH2COOCH3 (63.0 g; 0.143 mole), KOH (11.0 g; 0.196 mole; pellets) isopropanol (22 mL) and deionized water (18 mL). The ensuing mixture was refluxed overnight, cooled to room temperature, yielding a solution of C4F9SO2N(C3H7)CH2CH2CH2COOK (108.6 g; 53.4% solids).

후처리

  1. customA round bottom flask fitted with a heating mantle and an overhead stirrer
  2. temperatureThe ensuing mixture was refluxed overnight

출처 및 근거

ORD 기록
ord-c6bb3c3d062546a381cd192cf04f39fd
출처 데이터셋
uspto-grants-2010_10
특허 번호
US07811978B2

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