HuagongsheHuagongshe Chemistry Print Report · For research reference only
2H-1,2-Oxazine, tetrahydro- → HCID 178482954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2H-1,2-Oxazine, tetrahydro- | HCID 142102 | — |
| Reactant | HCID 178482947 | HCID 178482947 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Solvent | 2(1H)-Pyrimidinone, tetrahydro-1,3-dimethyl- | HCID 81646 | — |
| Product | HCID 178482954 | HCID 178482954 | 39.6% |
Reaction Steps
The compound of the example is prepared by the procedure of Example 1 using 2 g of [1,2]oxazinane, and 0.5 g of 9-(2-bromo-acetylamino)-4,7-bis-dimethylamino-3,10,12,12a-tetrahydroxy-1,11-dioxo-1,4,4a,5,5a,6,11,12a-octahydro-naphthacene-2-carboxylic acid amide in 8 ml DMPU and 2 ml acetonitrile to give 0.2 g of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812008B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-f33f07d4d8e04157be8bc2c7935b65b2 |
| Source note | uspto-grants-2010_10 |