化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → Chroman-4-one O-methyl-oxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Chromanone | HCID 68110 | — |
| 反応物 | 7-(Tert-butyl)chroman-4-one | HCID 59548541 | — |
| 生成物 | Chroman-4-one O-methyl-oxime | HCID 54035320 | — |
反応手順
The title compound was prepared using the procedure as described in Example 1B, substituting chroman-4-one for the product of Example 1A. 1H NMR (300 MHz, d6-DMSO) δ 7.79 (dd, J=1.0 and 7.5 Hz, 1H), 7.28 (m, 1H), 6.90 (m, 2H), 4.18 (t, J 6.0 Hz, 2H), 3.90 (s, 3H, minor), 3.88 (s, 3H, major), 2.82 (t, J 6.0 Hz, 2H). MS (DCI/NH3) m/e 178 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07812019B2 |
| 出典データセット | uspto-grants-2010_10 |
| ORD ID | ord-6bb8e7844ebe46a2a78f5a1cd64b60a4 |
| 出典メモ | uspto-grants-2010_10 |