HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-dihydro-2H-1-benzopyran-3-amine hydrochloride → 2-Aminochroman
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-dihydro-2H-1-benzopyran-3-amine hydrochloride | HCID 205708 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Product | 2-Aminochroman | HCID 20627838 | — |
Reaction Steps
3-aminochroman hydrochloride (0.37 g, 2 mmol) was neutralized with aqueous sodium bicarbonate, extracted with diethyl ether, dried with magnesium sulfate, and the solvent evaporated to give 2-aminochroman.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812019B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-dd6ca09f5051474ba020f90b8fc7dde4 |
| Source note | uspto-grants-2010_10 |