5-ethoxy-benzothiazol-2-ylamine → HCID 86611016, compound

HRID 1159612Notes

Reaction equation

HRID 1159612 reaction equation
[CH3:1][C:2]1([CH3:15])[O:11][C:10]2[C:5](=[CH:6][C:7]([C:12]#[N:13])=[CH:8][CH:9]=2)[CH:4]2[O:14][CH:3]12.[CH2:16]([O:18][C:19]1[CH:20]=[CH:21][C:22]2[S:26][C:25]([NH2:27])=[N:24][C:23]=2[CH:28]=1)[CH3:17]>>[CH2:16]([O:18][C:19]1[CH:20]=[CH:21][C:22]2[S:26][C:25]([NH:27][CH:4]3[C:5]4[C:10](=[CH:9][CH:8]=[C:7]([C:12]#[N:13])[CH:6]=4)[O:11][C:2]([CH3:15])([CH3:1])[CH:3]3[OH:14])=[N:24][C:23]=2[CH:28]=1)[CH3:17]

Participants

3

Reactant 2

HCID 8212115-ethoxy-benzothiazol-2-ylamineHCID 108673602,2-Dimethyl-3,4-epoxy-6-cyanochroman

Product 1

HCID 86611016HCID 86611016, compound

Procedure

Following the procedure in Example 1, using (±)-2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-carbonitrile and 5-ethoxy-benzothiazol-2-ylamine as starting material, the title compound was prepared as a white solid.

Sources & evidence

ORD record
ord-4739ccf666674966a0aa406fda63c42a
Source dataset
uspto-grants-2010_10
Patent number
US07812183B2

Reaction notes

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